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Basic One-and Two-Dimensional NMR Spectroscopy

Out of Print

By: H Friebolin

430 pages, Figs

John Wiley & Sons

Paperback | Dec 2005 | #154520 | ISBN: 3527312331
Out of Print Details

About this book

A classic among NMR textbooks, this thoroughly enlarged and updated fourth edition now also includes: Polymer solid state NMR; Analysis of biopolymers; Applications of Magnetic Resonance Tomography and Magnetic Resonance Spectroscopy.

If this reviewer had to choose one book as a reference for using nuclear magnetic resonance (NMR) spectroscopy, or one course resource to introduce (NMR) spectroscopy, this would be it. (CHOICE, December 2005) "...a comprehensive text for graduate students, although the book would also make an interesting reference for an organic chemistry library." (Journal of Natural Products, October 2005) From reviews of previous editions: "Another paperback that I would advise students to buy...[it] can be recommended for general purchase by all chemists." (New Scientist)


1 The Physical Basis of NMR Spectroscopy.1.1 Introduction.1.2 Nuclear Angular Momentum and Magnetic Moment.1.3 Nuclei in a Static Magnetic Field.1.4 Basic Principles of the NMR Experiment.1.5 The Pulsed NMR Method.1.6 Spectral Parameters: a Brief Survey.1.7 "Other" Nuclides.1.8 Bibliography for Chapter 1.2 The Chemical Shift.2.1 Introduction.2.2 1H Chemical Shifts of Organic Compounds.2.3 13C Chemical Shifts of Organic Compounds.2.4 Relationships between the Spectrum and the Molecular Structure.2.5 Chemical Shifts of "Other" Nuclides.2.6 Bibliography for Chapter 2.3 IndirectSpin-Spin Coupling.3.1 Introduction.3.2 H,H Coupling Constants and Chemical Structure.3.3 C,H Coupling Constants and Chemical Structure.3.4 C,C Coupling Constants and Chemical Structure.3.5 Correlations between C,H and H,H Coupling Constants.3.6 Coupling Mechanisms.3.7 Couplings of "Other" Nuclides (Heteronuclear Couplings).3.8 Bibliography for Chapter 3.4 Spectrum Analysis and Calculations.4.1 Introduction.4.2 Nomenclature.4.3 Two-Spin Systems.4.4 Three-Spin Systems.4.5 Four-Spin Systems.4.6 Spectrum Simulation and Iteration.4.7 Analysis of 13C NMR Spectra.4.8 Bibliography for Chapter 4.5 Double Resonance Experiments.5.1 Introduction.5.2 Spin Decoupling in 1HNMR Spectroscopy.5.3 Spin Decoupling in 13C NMR Spectroscopy.5.4 Bibliography for Chapter 5.6 Assignment of 1H and 13C Signals.6.1 Introduction.6.2 1HNMR Spectroscopy.6.3 13C NMR Spectroscopy.6.4 Computer-aided Assignment of 13C NMR Spectra.6.5 Bibliography for Chapter 6.7 Relaxation.7.1 Introduction.7.2 Spin-Lattice Relaxation of 13C Nuclei (T1).7.3 Spin-Spin Relaxation (T2).7.4 Bibliography for Chapter 7.8 One-Dimensional NMR Experiments using Complex Pulse Sequences.8.1 Introduction.8.2 Basic Techniques Using Pulse Sequences and Pulsed Field Gradients.8.3 The J-Modulated Spin-Echo Experiment.8.4 The Pulsed Gradient Spin-Echo Experiment.8.5 Signal Enhancement by Polarization Transfer.8.6 The DEPT Experiment.8.7 The Selective TOCSY Experiment.8.8 The One-Dimensional INADEQUATE Experiment.8.9 Bibliography for Chapter 8.9 Two-Dimensional NMR Spectroscopy.9.1 Introduction.9.2 The Two-Dimensional NMR Experiment.9.3 Two-Dimensional J-Resolved NMR Spectroscopy.9.4 Two-Dimensional Correlated NMR Spectroscopy.9.5 The Two-Dimensional INADEQUATE Experiment.9.6 Summary of Chapters 8 and 9.9.7 Bibliography for Chapter 9.10 The Nuclear Overhauser Effect.10.1 Introduction.10.2 Theoretical Background.10.3 Experimental Aspects.10.4 Applications.10.5 Bibliography for Chapter 10.11 Dynamic NMR Spectroscopy (DNMR).11.1 Introduction.11.2 Quantitative Calculations.11.3 Applications.11.4 Bibliography for Chapter 11.12 Shift Reagents.12.1 Lanthanide Shift Reagents (LSRs).12.2 Chiral Lanthanide Shift Reagents.12.3 Chiral Solvents.12.4 Bibliography for Chapter 12.13 Macromolecules.13.1 Introduction.13.2 Synthetic Polymers.13.3 Biopolymers.13.4 Bibliography for Chapter 13.14 NMR Spectroscopy in Biochemistry and Medicine.14.1 Introduction.14.2 Elucidating Reaction Pathways in Biochemistry.14.3 High-Resolution in vivo NMR Spectroscopy.14.4 Magnetic Resonance Tomography.14.5 Bibliography for Chapter 14.Subject Index.Index of Compounds.

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