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Experiments in Organic Chemistry

TextbookHandbook / ManualOut of Print

By: William Moore and Anthony Winston

McGraw Hill

Paperback | Dec 1996 | #93462 | ISBN: 0070430527
Out of Print Details

About this book

Provides an investigative approach for doing hands-on experimental work, comprising largely non traditional methods.


1 Safety in the Laboratory2 Introduction3 Melting Points4 Crystallization5 Distillation6 Gas Chromatography7 Thin-Layer Chromatography8 Extraction: Separation of an Unknown Mixture9 An Introuction to Stereochemistry: Use of Molecular Models10 Infared Spectroscopy11 Nuclear Magnetic Resonance Spectroscopy12 Assignment of Structure by IR and 1H-NMR Spectroscopy13 Preparative Scale GLC. Separation of Carvone and Limonene from Caroway Seed Oil14 SN1 and SN2 Reactions15 E2 Elimination Reactions, Dehydrobromination of the Byutyl Bromides, C4H9Br16 Elimination Reaction, Dehydration of Butyl Alcohols17 Hydroboration-Oxidation of Alkenes18 Reduction of Ketones to Alcohols with Sodium Borohydride19 Stereospecific Bromination of cis- and trans-Stilbene20 Diphenylacetylene and (E)-1,2-Dibromostilbene21 Addition Polymerization22 The Diels-Alder Reaction23 Aromatic Substitution I: Bromination of Aniline, Acetanilide, and Phenol24 Aromatic Substitution II: Nitration of Methyl Benzoate: Relative Reactivity of Aromatic Compounds: A Competitive Nitration25 The Grignard Reaction: The Synthesis of Triphenylmethanol26 Chromic Acid Oxidation of Para-Nitrotoluene to Para-Nitrobenzoic Acid27 Oxidation of Alcohols by a Chromate-Impregnated Resin: Following a Reaction by TLC28 The Haloform Reaction. Oxidation of Aryl Methyl Ketones to Aromatic Carboxylic Acids29 Synthesis of Isopentyl Acetate by Fischer Esterification30 Acetylation: Aspirin and N-Acetylanthranilic Acid31 Preparation of a Liquid Crystal: The Enol Acetate of 4-Cholestene-3-one32 The Claisen-Schmidt Reaction: Benzalacetone and Dibenzalacetone33 Aryldiazonium Ion Reactions: Formation, Displacement, Coupling34 Dyes Produced by Diazo Coupling and Diazo Imaging35 Imaging Dyes in Color Photography36 Qualitative Organic Analysis. Part 1: Preliminary Measurements and Classification Tests37 Qualitative Organic Analysis. Part 2: Prepartion of Derivatives and Final Identification38 Tables of Physical Properties of Compounds and their Derivatives Appendix

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