The development of problem-solving skills is a key element in chemistry courses. This work seeks to enhance these skills. It features a variety of problems, broadly based in analytical chemistry, developed in collaboration with universities and incorporating industrial ideas. Each of the 55 problems is complete with a solution and a guide for tutors. With subject matter ranging from gravimetric analysis to interpretation of spectroscopic data, the content should be suitable for use as group exercises in tutorials or for individual learning.